7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester

Base Information

Chemical Name:7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester
CAS No.:262278-27-3
Molecular Formula:C₁₈H₁₅NO₄
Molecular Weight:309.321
Hs Code.:

Synonyms:

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Chemical Property of 7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester

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Technology Process of 7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester

There total 4 articles about 7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 262278-27-3
7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / ammonium chloride; dimethyl sulfoxide

2: m-chloroperoxybenzoic acid; acetic anhydride / methanol; dichloromethane; sodium hydrogencarbonate; acetone

3: manganese dioxide; potassium carbonate / methanol; dichioromethane; dichloromethane

4: PTSA / tetrahydrofuran; NaH; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; ethyl acetate

With manganese dioxide; m-chloroperoxybenzoic acid; NaH; acetic anhydride; potassium carbonate; PTSA; In tetrahydrofuran; methanol; dichioromethane; NaH; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; ammonium chloride; sodium hydrogencarbonate; dimethyl sulfoxide; ethyl acetate; acetone;

Reference yield:

: 63793-98-6
5-benzyloxy-2-methyl-pyridine

: 262278-27-3
7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: m-chloroperoxybenzoic acid; acetic anhydride / methanol; dichloromethane; sodium hydrogencarbonate; acetone

2: manganese dioxide; potassium carbonate / methanol; dichioromethane; dichloromethane

3: PTSA / tetrahydrofuran; NaH; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; ethyl acetate

With manganese dioxide; m-chloroperoxybenzoic acid; acetic anhydride; potassium carbonate; PTSA; In tetrahydrofuran; methanol; dichioromethane; NaH; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; sodium hydrogencarbonate; ethyl acetate; acetone;

Reference yield:

: 59781-10-1
2-acetoxymethyl-5-benzyloxy pyridine

: 262278-27-3
7-benzyloxy-4-oxo-4H-quinolizine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: manganese dioxide; potassium carbonate / methanol; dichioromethane; dichloromethane

2: PTSA / tetrahydrofuran; NaH; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; ethyl acetate

With manganese dioxide; potassium carbonate; PTSA; In tetrahydrofuran; methanol; dichioromethane; NaH; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; ethyl acetate;