1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid
CAS No.:145398-23-8
Molecular Formula:C₇H₈O₃S*C₁₄H₁₄F₁₇NO₃
Molecular Weight:739.448
Hs Code.:

Synonyms:

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Chemical Property of 1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

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Technology Process of 1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

There total 3 articles about 1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 135462-67-8
Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester

: 111-42-2
2,2'-iminobis[ethanol]

: 145398-23-8
1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

Guidance literature:: In ethanol; at 60 ℃; for 48h;

Reference yield:

: 55118-40-6
1H,1H,2H-perfluorodecane-1,2-diol

: 145398-23-8
1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / diethyl ether / 1) 0 deg C, 2 h, 2) 40 deg C, 72 h

2: 82 percent / ethanol / 48 h / 60 °C

With pyridine; In diethyl ether; ethanol;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 145398-23-8
1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / diethyl ether / 1) 0 deg C, 2 h, 2) 40 deg C, 72 h

2: 82 percent / ethanol / 48 h / 60 °C

With pyridine; In diethyl ether; ethanol;