Technology Process of C15H15BrO2
There total 5 articles about C15H15BrO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diisobutylaluminum hydride;
In
toluene;
at -78 - 0 ℃;
for 4.5h;
DOI:10.1039/b703373g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.9 g / (bis)-triphenylphosphine palladium (II) chloride / pentane; tetrahydrofuran / 16 h / Heating
2: 75 percent / tetra-n-butylammonium fluoride; p-toluenesulphonic acid / tetrahydrofuran / 12 h / 0 - 20 °C
3: 85 percent / triphenylphosphine; carbon tetrabromide / CH2Cl2 / 0.5 h / 0 °C
4: di-iso-butylaluminium hydride / toluene / 4.5 h / -78 - 0 °C
With
diisobutylaluminum hydride; carbon tetrabromide; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triphenylphosphine;
(bis)-triphenylphosphine palladium (II) chloride;
In
tetrahydrofuran; dichloromethane; toluene; pentane;
1: Stille coupling reaction;
DOI:10.1039/b703373g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.9 g / (bis)-triphenylphosphine palladium (II) chloride / pentane; tetrahydrofuran / 16 h / Heating
2: 75 percent / tetra-n-butylammonium fluoride; p-toluenesulphonic acid / tetrahydrofuran / 12 h / 0 - 20 °C
3: 85 percent / triphenylphosphine; carbon tetrabromide / CH2Cl2 / 0.5 h / 0 °C
4: di-iso-butylaluminium hydride / toluene / 4.5 h / -78 - 0 °C
With
diisobutylaluminum hydride; carbon tetrabromide; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triphenylphosphine;
(bis)-triphenylphosphine palladium (II) chloride;
In
tetrahydrofuran; dichloromethane; toluene; pentane;
1: Stille coupling reaction;
DOI:10.1039/b703373g