C₆H₁₀(NP(C₆H₅)3)2

Base Information

Chemical Name:C₆H₁₀(NP(C₆H₅)3)2
CAS No.:207595-23-1
Molecular Formula:C₄₂H₄₀N₂P₂
Molecular Weight:634.741
Hs Code.:

C<sub>6</sub>H<sub>10</sub>(NP(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆H₁₀(NP(C₆H₅)3)2

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Technology Process of C₆H₁₀(NP(C₆H₅)3)2

There total 1 articles about C₆H₁₀(NP(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 1034-39-5
dibromotriphenylphosphorane

: 207595-23-1
C₆H₁₀(NP(C₆H₅)3)2

Guidance literature:: DOI:10.1039/a709023d

Reference yield: 88.0%

: di-μ-chlorido-bis(η3-1,3-diphenylallyl)dipalladium(II)

: 2923-28-6
silver trifluoromethanesulfonate

: 207595-23-1
C₆H₁₀(NP(C₆H₅)3)2

: ((C₆H₁₀(NP(C₆H₅)3)2)Pd(C₆H₅CHCHCHC₆H₅))⁽¹⁺⁾*CF₃SO₃^(1-)=((C₆H₁₀(NP(C₆H₅)3)2)Pd(C₆H₅CHCHCHC₆H₅))(CF₃SO₃)

: silver(I) chloride

Guidance literature:: In dichloromethane; under Ar atm. AgTfO was added to CH2Cl2 soln. of (Pd(η3-PhCHCHCHPh)Cl)2 and ligand at room temp., mixt. was stirred for 1 h in the dark; AgCl was filtered off, solvent was removed under vac., residue was crystd. from CH2Cl2-Et2O soln. at room temp.; elem. anal.;
DOI:10.1021/om990786d

Reference yield: 81.0%

: bis(η3-allyl-μ-chloropalladium(II))

: 2923-28-6
silver trifluoromethanesulfonate

: 207595-23-1
C₆H₁₀(NP(C₆H₅)3)2

: (C₆H₁₀(NP(C₆H₅)3)2)Pd(C₃H₅)⁽¹⁺⁾*CF₃SO₃^(1-)*0.5O(C₂H₅)2=((C₆H₁₀(NP(C₆H₅)3)2)Pd(C₃H₅))CF₃SO₃*0.5O(C₂H₅)2

: silver(I) chloride

Guidance literature:: In dichloromethane; under Ar atm. AgTfO was added to CH2Cl2 soln. of (Pd(η3-C3H5)Cl)2 and ligand at room temp., mixt. was stirred for 1 h in the dark; AgCl was filtered off, solvent was removed under vac., residue was subjected to column chromy. on silica (CH2Cl2 then MeOH); elem. anal.;
DOI:10.1021/om990786d