N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate

Base Information

Chemical Name:N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate
CAS No.:693219-09-9
Molecular Formula:BF₄*C₄₁H₃₄Au₂NOP₂
Molecular Weight:1099.41
Hs Code.:

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Chemical Property of N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate

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Technology Process of N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate

There total 2 articles about N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 67215-70-7
(triphenylphosphine)gold(I) tetrafluoroborate

: 3902-84-9
potassium 2-oxo-2H-pyridin-1-ide

: 693219-09-9
N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate

Guidance literature:: In tetrahydrofuran; under N2 atm. ((Ph3P)Au)BF4 in THF was added dropwise to soln. potassium2-pyridinolate in THF and stirred for 1 h; react. mixt. was evapd. to dryness in vacuo, residue was extd. with CH2Cl2, filtered, concd., and pptd. with n-pentane; elem. anal.;
DOI:10.1016/j.ica.2003.11.030

Reference yield: 31.0%

: 14104-20-2
silver tetrafluoroborate

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 930-70-1
2-pyridone sodium salt

: 693219-09-9
N,O-bis[(triphenylphosphine)gold]-2-pyridinolate tetrafluoroborate

: silver(I) chloride

Guidance literature:: In tetrahydrofuran; under N2 atm. (Ph3P)AuCl was added to cooled at -78°C soln. AgBF4in THF and stirred for 1 h at -78°C, ppt. was filtered off, filt rate was added dropwise to soln. sodium 2-pyridinolate in THF and stirred for 1 h; react. mixt. was evapd. to dryness in vacuo, residue was extd. with CH2Cl2, filtered, concd., and pptd. with n-pentane, recrystn. from CH2Cl2 bylayering with pentane; elem. anal.;
DOI:10.1016/j.ica.2003.11.030