W(CO)5(4-hydroxyphenyl diphenylphosphine)

Base Information

Chemical Name:W(CO)5(4-hydroxyphenyl diphenylphosphine)
CAS No.:252245-48-0
Molecular Formula:C₂₃H₁₅O₆PW
Molecular Weight:602.192
Hs Code.:

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Chemical Property of W(CO)5(4-hydroxyphenyl diphenylphosphine)

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Technology Process of W(CO)5(4-hydroxyphenyl diphenylphosphine)

There total 1 articles about W(CO)5(4-hydroxyphenyl diphenylphosphine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 14040-11-0
tungsten hexacarbonyl

: 5068-21-3
4-(diphenylphosphanyl)phenol

: 252245-48-0
W(CO)5(4-hydroxyphenyl diphenylphosphine)

Guidance literature:: In methanol; Irradiation (UV/VIS); N2-atmosphere; irradiation of W-complex for 4.5 h, addn. of phosphine, stirring overnight at room temp.; filtration, evapn., washing (hexane), drying (vac.); elem. anal.;
DOI:10.1016/S0277-5387(99)00194-1

Reference yield: 68.0%

: 252245-48-0
W(CO)5(4-hydroxyphenyl diphenylphosphine)

: 128175-80-4
2,2-dichloro-4,4,6,6-bis[spiro(2',2''-dioxy-1'',1''-biphenyl)]cyclotriphosphazene

: ((CO)5W(P(C₆H₅)2C₆H₄O))2P₃N₃((OC₆H₄)2)2

Guidance literature:: With caesium carbonate; In tetrahydrofuran; N2-atmosphere; refluxing for 45 min; evapn., extn. (CH2Cl2), filtration, evapn.; elem. anal.;
DOI:10.1016/S0277-5387(99)00194-1

Reference yield: 24.0%

: 1832-07-1,25034-79-1
poly(dichlorophosphazene)

: 1806-29-7
2,2'-dihydroxybiphenyl

: 252245-48-0
W(CO)5(4-hydroxyphenyl diphenylphosphine)

: [(((CO)5W(PPh₂C₆H₄O))2PN)0.35(((C₆H₄O)2)PN)0.65]n

Guidance literature:: With potassium carbonate; caesium carbonate; In tetrahydrofuran; N2-atmosphere; refluxing (PNCl2)n, biphenole and K2CO3 for 6 h, addn. ofW-complex and Cs2CO3, refluxing for 16 h; pouring into H2O, washing (H2O), extn. (THF), pptn. (H2O), re-pptn. (THF:iPrOH, THF:petroleum ether), drying (vac.); elem. anal.;
DOI:10.1016/S0277-5387(99)00194-1