(2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol

Base Information

Chemical Name:(2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol
CAS No.:81408-48-2
Molecular Formula:C₂₁H₂₉N₅O
Molecular Weight:367.494
Hs Code.:

Synonyms:

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Chemical Property of (2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol

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Technology Process of (2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol

There total 6 articles about (2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81408-32-4
5-O-benzyl-1,2:3,4-di-O-isopropylidene-D-rhamnitol

: 81408-48-2
(2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / trifluoroacetic acid / H₂O / Ambient temperature

2: 78 percent / sodium metaperiodate, NaOH / H₂O / 16 h / Ambient temperature

3: 54 percent / tetrahydrofuran / 24 h / Heating

4: pyridine / 48 h / Ambient temperature

5: 1.) NaH / 1.) N,N-dimethylformamide, room temperature, 24 h, 2.) N,N-dimethylformamide, 50 deg C, 7 days

With pyridine; sodium hydroxide; sodium periodate; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; water;
DOI:10.1021/jo00132a039

Reference yield:

: 81408-33-5
5-O-benzyl-D-rhamnitol

: 81408-48-2
(2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / sodium metaperiodate, NaOH / H₂O / 16 h / Ambient temperature

2: 54 percent / tetrahydrofuran / 24 h / Heating

3: pyridine / 48 h / Ambient temperature

4: 1.) NaH / 1.) N,N-dimethylformamide, room temperature, 24 h, 2.) N,N-dimethylformamide, 50 deg C, 7 days

With pyridine; sodium hydroxide; sodium periodate; sodium hydride; In tetrahydrofuran; water;
DOI:10.1021/jo00132a039

Reference yield:

: 53346-05-7,41954-96-5,81445-44-5,81445-45-6
(R)-2-benzyloxypropanal

: 81408-48-2
(2R,3S)-3-(adenin-9-yl)-2-O-benzyl-2-nonanol

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / tetrahydrofuran / 24 h / Heating

2: pyridine / 48 h / Ambient temperature

3: 1.) NaH / 1.) N,N-dimethylformamide, room temperature, 24 h, 2.) N,N-dimethylformamide, 50 deg C, 7 days

With pyridine; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00132a039