gadolinium(III) sesquioxalate decahydrate

Base Information

• Chemical Name: gadolinium(III) sesquioxalate decahydrate
• CAS No.: 10171-51-4
• Molecular Formula: 3C₂O₄*2Gd*10H₂O
• Molecular Weight: 758.712
• Mol file: 10171-51-4.mol

Synonyms:

Chemical Property of gadolinium(III) sesquioxalate decahydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of gadolinium(III) sesquioxalate decahydrate

There total 10 articles about gadolinium(III) sesquioxalate decahydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

gadolinium(III) chloride hexahydrate + water (7732-18-5) + oxalic acid (144-62-7,97993-78-7) → gadolinium(III) sesquioxalate decahydrate (7100-54-1,10171-51-4,13082-73-0,22992-15-0)

Guidance literature:

at 50 ℃;

DOI:10.1039/d1dt00462j

Reference yield:

Dimethyl oxalate (553-90-2) → gadolinium(III) sesquioxalate decahydrate (7100-54-1,10171-51-4,13082-73-0,22992-15-0)

Guidance literature:

With nitric acid; In water; stirring, heating on water bath for 3 h, standing overnight at room temp.; filtrn., washed with ethanol, ether, dried for 24 h in air at room temp.;

DOI:10.1021/ac60133a015

Reference yield:

gadolinium(III) oxide + oxalic acid (144-62-7,97993-78-7) → gadolinium(III) sesquioxalate decahydrate (7100-54-1,10171-51-4,13082-73-0,22992-15-0)

Guidance literature:

With HCl; In water; Gd2O3 dissolved in HCl, oxalic acid added; filtered, washed with water, dried in air at 80 °C for 24 h;

DOI:10.1007/s10973-005-7209-3

upstream raw materials:

oxalic acid

gadolinium(III) chloride

Dimethyl oxalate

hydrogenchloride