3,3-Diphenyl-hexanedioic acid diethyl ester

Base Information

Chemical Name:3,3-Diphenyl-hexanedioic acid diethyl ester
CAS No.:157311-36-9
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:

Suppliers and Price of 3,3-Diphenyl-hexanedioic acid diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,3-Diphenyl-hexanedioic acid diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,3-Diphenyl-hexanedioic acid diethyl ester

There total 3 articles about 3,3-Diphenyl-hexanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: (E)-4,4-Diphenyl-6-trimethylsilanyloxy-hex-5-enoic acid ethyl ester

: 157311-36-9
3,3-Diphenyl-hexanedioic acid diethyl ester

Guidance literature:: With caro's acid; sulfuric acid; at 0 ℃; for 6h; Yield given;
DOI:10.1021/jo00097a070

Reference yield:

: 119-61-9
benzophenone

: 157311-36-9
3,3-Diphenyl-hexanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) diisopropylamine, butyllithium, 2.) citric acid / 1.) THF, hexane, 0 deg C, 15 min; -78 deg C to r.t., 3 h, 2.) H₂O, r.t., overnight

2: 1.) ZnCl₂, 2.) CuBr*SMe₂, HMPA / 1.) ether, reflux, 2 h, 2.) THF, 0 deg C, 5 min; r.t., 3 h

3: H₂SO₅, conc. H₂SO₄ / 6 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; caro's acid; copper(I) bromide dimethylsulfide complex; sulfuric acid; diisopropylamine; citric acid; zinc(II) chloride;
DOI:10.1021/jo00097a070

Reference yield:

: 1210-39-5
3,3-diphenyl-2-propenal

: 157311-36-9
3,3-Diphenyl-hexanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ZnCl₂, 2.) CuBr*SMe₂, HMPA / 1.) ether, reflux, 2 h, 2.) THF, 0 deg C, 5 min; r.t., 3 h

2: H₂SO₅, conc. H₂SO₄ / 6 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; caro's acid; copper(I) bromide dimethylsulfide complex; sulfuric acid; zinc(II) chloride;
DOI:10.1021/jo00097a070