(2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

Base Information

Chemical Name:(2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide
CAS No.:1064668-19-4
Molecular Formula:C₃₄H₄₇NO₂
Molecular Weight:501.753
Hs Code.:

(2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

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Chemical Property of (2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

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Technology Process of (2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

There total 1 articles about (2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1107-26-2,4172-46-7
trans-β-apo-8'-carotenal

: 129986-67-0
N-methoxy-N-methyl-2-(triphenylphosphoranylidene)acetamide

: 1064668-19-4
(2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

Guidance literature:: In benzene; at 65 ℃; for 144h;
DOI:10.1021/jp994436g

Reference yield:

: 1064668-19-4
(2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

: 5056-13-3
6'-Apo-β-caroten-6'-al

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1021/jp994436g

Reference yield:

: 1064668-19-4
(2E,4E,6E,8E,10E,12E,14E,16E,18E)-4,8,13,17-Tetramethyl-19-(2,6,6-trimethyl-cyclohex-1-enyl)-nonadeca-2,4,6,8,10,12,14,16,18-nonaenoic acid methoxy-methyl-amide

: 4'-Apo-β-caroten-4'-al

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / tetrahydrofuran / 1 h / -78 °C

2: benzene / 144 h / 65 °C

3: DIBAL-H / tetrahydrofuran / 1 h / -78 °C

With diisobutylaluminium hydride; In tetrahydrofuran; benzene; 1: Reduction / 2: Condensation / 3: Reduction;
DOI:10.1021/jp994436g