{Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄

Base Information

Chemical Name:{Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄
CAS No.:80084-46-4
Molecular Formula:C₄₁H₅₃MnN₂O₇P₃*ClO₄
Molecular Weight:933.191
Hs Code.:

{Mn(CO)(bipy)(P(OEt)2Ph)3}ClO<sub>4</sub>

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Chemical Property of {Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄

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Technology Process of {Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄

There total 1 articles about {Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79982-35-7
cis,trans-{Mn(CO)2(bipy)(P(OEt)2Ph)2}ClO₄

: 1638-86-4
diethyl phenylphosphonite

: 80084-46-4
{Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄

Guidance literature:: In acetone; Irradiation (UV/VIS); under N2 for 7.5 h; the soln. was evapd. to dryness, the residue was washed with diethyl ether, the product recrystd. from CH2Cl2/ethanol; elem. anal.;
DOI:10.1016/0022-328X(81)85010-3

Reference yield:

: 80084-46-4
{Mn(CO)(bipy)(P(OEt)2Ph)3}ClO₄

: cis,cis-{Mn(CO)2(bipy)(P(OEt)2Ph)2}ClO₄

Guidance literature:: With CO; In acetone; Irradiation (UV/VIS); CO was bubbled for 1 h through the soln. of the complex exposed to UV light under N2; the soln. was evapd. to dryness and the residue was washed with diethyl ether to remove the free ligand, acetone was added and the treatment was repeated every 1/2 h (IR control), ethanol was added and the solvents were evapd. in vac.; elem anal.;
DOI:10.1016/0022-328X(81)85010-3