N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid

Base Information

• Chemical Name: N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid
• CAS No.: 151414-66-3
• Molecular Formula: C₁₅H₂₆ClNO₂Si₂
• Molecular Weight: 344.001

Synonyms:

Chemical Property of N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid

There total 2 articles about N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Chloro(chloromethyl)dimethylsilane (1719-57-9) + 2-trimethylsilyloxy-2-phenylacetic acid N-methylamide (151414-64-1) → N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid (151414-66-3)

Guidance literature:

With triethylamine; In benzene;

Reference yield:

N-methyl-2-hydroxy-2-phenylethanamide (65645-88-7,89843-35-6,96392-41-5,2019-72-9) → N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid (151414-66-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent

2: Et₃N / benzene

With triethylamine; In benzene;

Reference yield: 71.0%

N-methyl-N-amide of 2-trimethylsilyloxy-2-phenylacetic acid (151414-66-3) → 2,2,4-trimethyl-6-phenyl-1-oxa-4-aza-2-silacyclohexan-5-one (151414-68-5)

Guidance literature:

Heating;

upstream raw materials:

Chloro(chloromethyl)dimethylsilane

2-trimethylsilyloxy-2-phenylacetic acid N-methylamide

N-methyl-2-hydroxy-2-phenylethanamide

Downstream raw materials:

2,2,4-trimethyl-6-phenyl-1-oxa-4-aza-2-silacyclohexan-5-one

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