(C₅H₅)W(CO)2(CS)Pb(C₆H₅)3

Base Information

Chemical Name:(C₅H₅)W(CO)2(CS)Pb(C₆H₅)3
CAS No.:74989-75-6
Molecular Formula:C₂₆H₂₀O₂PbSW
Molecular Weight:787.56
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)W(CO)2(CS)Pb(C<sub>6</sub>H<sub>5</sub>)3

Synonyms:

Suppliers and Price of (C₅H₅)W(CO)2(CS)Pb(C₆H₅)3

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (C₅H₅)W(CO)2(CS)Pb(C₆H₅)3

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (C₅H₅)W(CO)2(CS)Pb(C₆H₅)3

There total 1 articles about (C₅H₅)W(CO)2(CS)Pb(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 74989-73-4
N(C₄H₉)4⁽¹⁺⁾*W(C₅H₅)(CO)2CS^(1-)=N(C₄H₉)4W(C₅H₅)(CO)2CS

: 1153-06-6
triphenyllead(IV) chloride

: 74989-75-6
cis-CpW(CO)2(CS)PbPh₃

Guidance literature:: In tetrahydrofuran; (N2); Ph3PbCl was added to soln. of W complex at 0°C; after 10 min mixt. was filtered through Celite and evapd. in vac., slurry in CH2Cl2 was chromd. (Florisil, CH2Cl2); eluate was concd., diluted with hexane and evapd. in vac.; recrystn. from CH2Cl2/hexane at -20°C; elem. anal.;
DOI:10.1016/S0022-328X(00)88554-X

Reference yield: 30.0%

: 74989-75-6
(C₅H₅)W(CO)2(CS)Pb(C₆H₅)3

: 74-89-5
methylamine

: (C₅H₅)W(CO)2(CNCH₃)Pb(C₆H₅)3

Guidance literature:: With mercury; In tetrahydrofuran; W-complex was placed in tube, evacuated, filled with N2, THF was injected, Hg was bubbled, ligand was introduced into tube, allowed to bubble through the soln. for 15 min, vessel was pressurized to ca. 2 atm with ligand; soln. was stirred for 20 h at 50°C, cooled to room temp., evapd.under reduced pressure, residue extd. with benzene, eluted on alumina column with benzene, eluate was collected, evapd., crystd. from CH2Cl2/hexane at -20°C; elem. anal.;