[PtCl(Me)(diacetyl bis(phenylimine))]

Base Information

Chemical Name:[PtCl(Me)(diacetyl bis(phenylimine))]
CAS No.:199284-94-1
Molecular Formula:C₁₇H₁₉ClN₂Pt
Molecular Weight:481.884
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [PtCl(Me)(diacetyl bis(phenylimine))]

Chemical Property:

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Technology Process of [PtCl(Me)(diacetyl bis(phenylimine))]

There total 1 articles about [PtCl(Me)(diacetyl bis(phenylimine))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2,3-dimethyl-1,4-diphenyl-1,4-diazabuta-1,3-diene

: PtCl(methyl)(dimethyl sulfide)2

: 199284-94-1
[PtCl(Me)(diacetyl bis(phenylimine))]

Guidance literature:: In diethyl ether; addn. of 1.2 equiv. of ligand to suspension of Pt-complex, stirring for 48 h at room temp.; collection, washing (Et2O), drying (vac.); NMR spectroscopy;
DOI:10.1021/om970428f

Reference yield: 99.0%

: 14104-20-2
silver tetrafluoroborate

: 199284-94-1
[PtCl(Me)(diacetyl bis(phenylimine))]

: 75-05-8,26809-02-9
acetonitrile

: (Pt(CH₃)(CH₃CN)(N₂C₂(CH₃)2(C₆H₅)2))⁽¹⁺⁾*BF₄^(1-)=(Pt(CH₃)(CH₃CN)(N₂C₂(CH₃)2(C₆H₅)2))(BF₄)

: silver(I) chloride

Guidance literature:: In tetrahydrofuran; under N2 atm. Pt complex was added to soln. AgBF4 and MeC in THF and stirred for 5 min; solvent was removed under vac., residue was extd. with CH2Cl2, solvent was removed in vacuo; elem. anal.;
DOI:10.1021/ic011059p

Reference yield: 80.0%

: 14104-20-2
silver tetrafluoroborate

: 187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4
propene

: 199284-94-1
[PtCl(Me)(diacetyl bis(phenylimine))]

: 199284-86-1
[Pt(Me)(diacetyl bis(phenylimine))(propylene)](BF₄)

Guidance literature:: In dichloromethane; byproducts: AgCl; mixing AgBF4 and excess of propylene, addn. of Pt-complex at 273 K, stirring for 48 h at room temp.; filtration off of AgCl (Celite), concn., crystn. on addn. of MePh and standing at 277 K, washing (MePh, pentane), drying (vac.); NMR spectroscopy;
DOI:10.1021/om970428f