6H-Cyclohepta(b)quinolin-11-amine, 7,8,9,10-tetrahydro-N-hexyl-, monohydrochloride

Base Information

• Chemical Name: 6H-Cyclohepta(b)quinolin-11-amine, 7,8,9,10-tetrahydro-N-hexyl-, monohydrochloride
• CAS No.: 108154-83-2
• Molecular Formula: C₂₀H₂₈N₂*ClH
• Molecular Weight: 332.917
• DSSTox Substance ID: DTXSID40148450

Synonyms:7,8,9,10-Tetrahydro-N-hexyl-6H-cyclohepta(b)quinolin-11-amine hydrochloride;6H-Cyclohepta(b)quinolin-11-amine, 7,8,9,10-tetrahydro-N-hexyl-, monohydrochloride;108154-83-2;NIOSH/GU3516200;DTXSID40148450;LS-56049;LS-56099;GU35162000;6H-Cyclohepta(b)quinoline, 7,8,9,10-tetrahydro-11-(hexylamino)-, monohydrochloride;7,8,9,10-Tetrahydro-11-(hexylamino)-6H-cyclohepta(b)quinoline monohydrochloride

Chemical Property of 6H-Cyclohepta(b)quinolin-11-amine, 7,8,9,10-tetrahydro-N-hexyl-, monohydrochloride

Chemical Property:

• Vapor Pressure: 7.43E-09mmHg at 25°C
• Boiling Point: 465.8°C at 760 mmHg
• Flash Point: 235.5°C
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 332.2019266
• Heavy Atom Count: 23
• Complexity: 317

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCNC1=C2CCCCCC2=NC3=CC=CC=C31.Cl

Technology Process of 6H-Cyclohepta(b)quinolin-11-amine, 7,8,9,10-tetrahydro-N-hexyl-, monohydrochloride

There total 2 articles about 6H-Cyclohepta(b)quinolin-11-amine, 7,8,9,10-tetrahydro-N-hexyl-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

10-chloro-2,3,4,5-tetrahydro-1H-cyclohepta[1,2-b]quinoline (5778-71-2) + hexan-1-amine (111-26-2) → 4-n-Hexylamino-2,3-pentamethylenequinoline hydrochloride (108154-83-2)

Guidance literature:

With phenol; at 145 - 150 ℃; for 20h;

Reference yield:

1-Chlorohexane (544-10-5) + 7,8,9,10-tetrahydro-6H-cyclohepta[b]quinolin-11-ylamine (5778-86-9) → 4-n-Hexylamino-2,3-pentamethylenequinoline hydrochloride (108154-83-2)

Guidance literature:

With sodium hydride; Multistep reaction; 1.) DMF, 90 deg C, 1 h, 2.) DMF, 90 deg C, 3 h;

upstream raw materials:

10-chloro-2,3,4,5-tetrahydro-1H-cyclohepta[1,2-b]quinoline

hexan-1-amine

1-Chlorohexane

7,8,9,10-tetrahydro-6H-cyclohepta[b]quinolin-11-ylamine

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