methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate

Base Information

Chemical Name:methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate
CAS No.:164937-05-7
Molecular Formula:C₃₆H₅₀I₂O₇
Molecular Weight:848.598
Hs Code.:

methyl hydrogen o,o'-diiodo-11,11'-<carbonylbis(p-phenylenoxy)>bisundecanoate

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Chemical Property of methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate

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Technology Process of methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate

There total 1 articles about methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 164937-00-2
dimethyl 11,11'-bisundecanoate

: o,o'-diiodo-11,11'-bisundecanoic acid

: 164937-05-7
methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate

: 164937-04-6
dimethyl o,o'-diiodo-11,11'-bisundecanoate

Guidance literature:: With Iodine monochloride; In acetic acid; at 80 ℃; for 2.75h;

Reference yield: 100.0%

: 67-56-1
methanol

: 164937-05-7
methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate

: 164937-04-6
dimethyl o,o'-diiodo-11,11'-bisundecanoate

Guidance literature:: With thionyl chloride; for 0.25h; Heating;

Reference yield:

: 164937-05-7
methyl hydrogen o,o'-diiodo-11,11'-bisundecanoate

: 164936-96-3
3,3'-(11,11'-bisundecanoyl)bisthiazolidine-2-thione

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / SOCl₂ / 0.25 h / Heating

2: 92 percent / H₂, NaOAc / 10percent Pd/C / tetrahydrofuran; methanol / 2 h / Ambient temperature

3: 92 percent / KOH / aq. ethanol; tetrahydrofuran / 5 h / Heating

4: dicyclohexylcarbodiimide (DCC), pyridine

With pyridine; potassium hydroxide; thionyl chloride; hydrogen; sodium acetate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;