[(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid

Base Information

Chemical Name:[(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid
CAS No.:889098-91-3
Molecular Formula:C₁₇H₂₇NO₃
Molecular Weight:293.406
Hs Code.:

Synonyms:

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Chemical Property of [(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid

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Technology Process of [(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid

There total 1 articles about [(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 96-76-4
2,4-di-tert-Butylphenol

: 56-40-6,18875-39-3,25718-94-9
glycine

: 889098-91-3
[(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid

Guidance literature:: In water;
DOI:10.1002/ejic.200500601

Reference yield: 60.0%

: 889098-91-3
[(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid

: 7631-95-0
sodium molybdate dihydrate

: 15690-63-8,64704-31-0,7647-17-8
cesium chloride

: Cs₂Mo₂O₅-bis[(3,5-di-tert-butyl-2-oxybenzyl)amino]acetate(H₂O)

Guidance literature:: In methanol; water; aq. soln. of Na2MoO4*2H2O added to soln. of ligand in CH3OH, mixt. stirred for 6 h, CsCl added, soln. stirred for 1 h; crystd. after 10 d;
DOI:10.1002/ejic.200500601

Reference yield: 54.0%

: 889098-91-3
[(3,5-di-tert-butyl-2-hydroxybenzyl)amino]acetic acid

: 7631-95-0
sodium molybdate dihydrate

: [(sodium)4(H2O)4(μ-H2O)2][manganese(II)((Mo2O5(2-(3,5-di-tert-butyl-2-hydroxybenzylamino)acetate(-H))2]2

Guidance literature:: In methanol; water; aq. soln. of Na2MoO4*2H2O added to soln. of ligand in CH3OH, mixt. stirred for 3 h; crystd. overnight, crystals filtered off, washed with H2O, dried under vac., recrystd. from CH3OH/CH3CN; elem. anal.;
DOI:10.1002/ejic.200500601