4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.1^3.7.1^9,13.1^15,19]-octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene

Base Information

• Chemical Name: 4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.1^3.7.1^9,13.1^15,19]-octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene
• CAS No.: 1008753-85-2
• Molecular Formula: C₉₆H₁₂₈O₁₂
• Molecular Weight: 1474.07

Synonyms:

Chemical Property of 4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.1^3.7.1^9,13.1^15,19]-octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene

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Technology Process of 4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.1^3.7.1^9,13.1^15,19]-octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene

There total 1 articles about 4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.1^3.7.1^9,13.1^15,19]-octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

3,5-di-tert-butyl-4-hydroxybenzyl acetate (14387-17-8) + C-ethylcalix[4]resorcinarene (135971-85-6,1224192-66-8) → 4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.13.7.19,13.115,19]-octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene (1008753-85-2) + 2,4,6-tris(3,5-di-tert-butyl-4-hydroxybenzyl)resorcinol

Guidance literature:

With formic acid; In acetone; at 20 ℃; for 24h;

DOI:10.1007/s11172-009-0021-7

Reference yield: 64.0%

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.13.7.19,13.115,19]-octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene (1008753-85-2) + acetic anhydride (108-24-7) → C120H152O24

Guidance literature:

at 100 ℃; for 48h;

DOI:10.1134/S1070363207030206

Reference yield: 52.0%

methylphosphonic acid dichloroanhydride (676-97-1) + 4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetra(3,5-di-tert-butyl-4-hydroxybenzyl)-2,8,14,20-tetraethylpentacyclo[19.3.1.13.7.19,13.115,19]-octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene (1008753-85-2) → C100H132O16P4

Guidance literature:

With triethylamine; In acetonitrile; Heating;

DOI:10.1134/S1070363207030206

upstream raw materials:

3,5-di-tert-butyl-4-hydroxybenzyl acetate

C-ethylcalix[4]resorcinarene

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