H₃BP(C₆H₅)((CH₂)6CHCH₂)2

Base Information

Chemical Name:H₃BP(C₆H₅)((CH₂)6CHCH₂)2
CAS No.:709008-45-7
Molecular Formula:C₂₂H₃₈BP
Molecular Weight:344.328
Hs Code.:

H<sub>3</sub>BP(C<sub>6</sub>H<sub>5</sub>)((CH<sub>2</sub>)6CHCH<sub>2</sub>)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H₃BP(C₆H₅)((CH₂)6CHCH₂)2

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Technology Process of H₃BP(C₆H₅)((CH₂)6CHCH₂)2

There total 1 articles about H₃BP(C₆H₅)((CH₂)6CHCH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 13292-87-0
dimethyl sulfide borane

: 321991-73-5
di-oct-7-enyl-phenyl-phosphane

: 709008-45-7
H₃BP(C₆H₅)((CH₂)6CHCH₂)2

Guidance literature:: In tetrahydrofuran; (N2); charging of Schlenk flask with PPh((CH2)6CHCH2)2 and THF, cooling to -20°C (N2, acetone); addn. of H3B*SMe2; stirring for 1 h at -20°C and 30 min at room temp.; removal of solvent by rotary evapn. and oil-pump vac., filtration through neutral alumina using 1:1 v/v CH2Cl2-hexanes; removal of solvent by oil-pump vac., as oil; elem. anal.;
DOI:10.1039/b400156g

Reference yield:

: 709008-45-7
H₃BP(C₆H₅)((CH₂)6CHCH₂)2

: 709008-48-0
trans-[Pt(Cl)(C₆F₅)(PPh(CH₂)14)2]

Guidance literature:: Multi-step reaction with 3 steps

1: Grubbs catalyst first generation / dichloromethane

2: Wilkinson's catalyst / benzene

3: HNEt₂ / dichloromethane

With HNEt₂; Grubbs catalyst first generation; Wilkinson's catalyst; In dichloromethane; benzene;
DOI:10.1039/b400156g