[(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]

Base Information

Chemical Name:[(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]
CAS No.:262606-67-7
Molecular Formula:C₁₇H₂₀ClPPd
Molecular Weight:397.193
Hs Code.:

[(CH<sub>3</sub>CHCHCH<sub>2</sub>)PdCl(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)]

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Chemical Property of [(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]

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Technology Process of [(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]

There total 1 articles about [(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: bis[(1,2,3-η)-2-butenyl]di(μ-chloro)palladium(II)

: 1486-28-8
diphenyl(methyl)phosphine

: 262606-67-7
[(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]

Guidance literature:: In dichloromethane; in Schlenk tube; addn. of phosphine at -10°C, then stirring for 30 min at room temp.; filtration through Al2O3, concn. under reduced pressure, crystn. by layering with Et2O at room temp., drying crystals under vac.; elem. anal.;
DOI:10.1246/bcsj.73.453

Reference yield: 86.0%

: 262606-67-7
[(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]

: 13126-70-0
silver(I) formate

: 132884-85-6
formato(η3-1-methylallyl)(methyldiphenylphosphine)palladium(II)

Guidance literature:: In dichloromethane; under inert atmosphere; addn. of HCO2Ag to soln. of Pd complex at -40°C, stirring at -20°C for 2 h in the dark; filtration (celite, -50°C), evapn.;
DOI:10.1246/bcsj.73.453

Reference yield: 63.0%

: 262606-67-7
[(CH₃CHCHCH₂)PdCl(PCH₃(C₆H₅)2)]

: 563-63-3
silver(I) acetate

: 262606-68-8
acetato(η3-1-methylallyl)(methyldiphenylphosphine)palladium(II)

Guidance literature:: In dichloromethane; under inert atmosphere; addn. at -30°C, stirring at -10°Cfor 3 h in the dark; filtration (celite, room temp.); evapn.;
DOI:10.1246/bcsj.73.453