(C₅H₅)Mn(CO)2(C₅H₄FeC₅H₄PC₆H₅)

Base Information

• Chemical Name: (C₅H₅)Mn(CO)2(C₅H₄FeC₅H₄PC₆H₅)
• CAS No.: 315195-52-9
• Molecular Formula: C₂₃H₁₈FeMnO₂P
• Molecular Weight: 468.153

Synonyms:

Chemical Property of (C₅H₅)Mn(CO)2(C₅H₄FeC₅H₄PC₆H₅)

Chemical Property:

Purity/Quality:

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Technology Process of (C₅H₅)Mn(CO)2(C₅H₄FeC₅H₄PC₆H₅)

There total 1 articles about (C₅H₅)Mn(CO)2(C₅H₄FeC₅H₄PC₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1,1'-(ferrocenediyl)phenylphosphine + dicarbonyl(η(5)-cyclopentadienyl)manganese(THF) → (C5H5)Mn(CO)2(C5H4FeC5H4PC6H5) (315195-52-9)

Guidance literature:

In tetrahydrofuran; a mixt. in THF was stirred for 7 h (N2); the solvent was removed in vac., the residue was suspn. in hexane and CH2Cl2 was added, filtered, the solvent was removed in vac., the residue was dried in vac.; elem. anal.;

DOI:10.1021/om000453c

Reference yield: 74.0%

(C5H5)Mn(CO)2(C5H4FeC5H4PC6H5) (315195-52-9) → (C5H5)Mn(CO)2(C5H4FeC5H4PC6H5) (114610-49-0)

Guidance literature:

In tetrahydrofuran; Irradiation (UV/VIS); a soln. in THF was irradiated for 10 min at 0°C with mercury arc lamp (N2); filtered, the solvent was removed;

DOI:10.1021/om000453c

Reference yield: 29.0%

tetrakis(trimethylphosphine)platinum(0) (33937-27-8) + dichloromethane (75-09-2) + (C5H5)Mn(CO)2(C5H4FeC5H4PC6H5) (315195-52-9) → C5H5Mn(CO)2P(C6H5)(C5H4)2FePt(P(CH3)3)2*CH2Cl2

Guidance literature:

In toluene; a mixt. in toluene was heated at 70°C for 6 h (N2); the solvent was removed in vac., chromd. on silica gel column (CH2Cl2-hexane); elem. anal.;

DOI:10.1021/om010797i

Downstream raw materials:

(C₅H₅)Mn(CO)2(C₅H₄FeC₅H₄PC₆H₅)

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