(Rp)-ortho-diphenylphosphanylferrocene carboxylic acid

Base Information

Chemical Name:(Rp)-ortho-diphenylphosphanylferrocene carboxylic acid
CAS No.:149095-48-7
Molecular Formula:C₂₃H₁₉FeOP
Molecular Weight:398.224
Hs Code.:

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Chemical Property of (Rp)-ortho-diphenylphosphanylferrocene carboxylic acid

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Technology Process of (Rp)-ortho-diphenylphosphanylferrocene carboxylic acid

There total 6 articles about (Rp)-ortho-diphenylphosphanylferrocene carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (C₅H₅)Fe(C₅H₃(P(C₆H₅)2)C(O)OCH(CH₂C(CH₂)CH(CH₃)2)CH₂CH(CH(CH₃)2)CH₂CHO)

: potassium hydroxide

: 149-73-5
trimethyl orthoformate

: 149095-48-7,1144039-25-7
(Rp)-ortho-diphenylphosphanylferrocene carboxylic acid

: 766528-45-4
(3S,5S)-3-isopropyl-1,1-dimethoxy-8-methyl-7-methylene-nonan-5-ol

Guidance literature:: With TsOH; In ethanol; Fe complex treated with HC(OMe)3 and TsOH in MeOH under heating; heated with KOH in EtOH;
DOI:10.1021/ja0467364

Reference yield: 87.0%

: 1094756-39-4
1-bromo-2-(diphenylphosphino)ferrocene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1144039-25-7,149095-48-7
(S)-α-(diphenylphosphino)ferrocenecarboxaldehyde

Guidance literature:: 1-bromo-2-(diphenylphosphino)ferrocene; With n-butyllithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h; Inert atmosphere; Schlenk technique; Glovebox;

N,N-dimethyl-formamide; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 1.5h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/ejic.201601440