Technology Process of CH2O2*C11H14N2O
There total 3 articles about CH2O2*C11H14N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N-Pmc-N'-allyl-4-methoxybenzamide;
With
trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid;
at 20 ℃;
for 4h;
formic acid;
In
methanol; ethyl acetate;
DOI:10.1055/s-0030-1260011
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium; lithium chloride / tetrahydrofuran / Inert atmosphere
1.2: 0.83 h / 0 °C / Inert atmosphere
2.1: 2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / 20 °C
2.2: 0.5 h / 20 °C
3.1: trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid / 4 h / 20 °C
With
trimethylsilyl trifluoromethanesulfonate; 2-chloro-1-methyl-pyridinium iodide; magnesium; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0030-1260011
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / 20 °C
1.2: 0.5 h / 20 °C
2.1: trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid / 4 h / 20 °C
With
trimethylsilyl trifluoromethanesulfonate; 2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1055/s-0030-1260011
