Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium

Base Information

Chemical Name:Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium
CAS No.:147363-24-4
Molecular Formula:C₇H₄NO₄*C₁₀H₁₂N
Molecular Weight:312.325
Hs Code.:

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Chemical Property of Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium

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Technology Process of Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium

There total 4 articles about Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 114640-73-2
N-methyl-1-hydroxy-1,2,3,4-tetrahydroisoquinoleine

: 62-23-7
4-nitro-benzoic acid

: 147363-24-4
Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium

Guidance literature:: In dichloromethane;
DOI:10.1016/S0040-4020(01)80311-2

Reference yield:

: 3230-65-7
3,4-dihydroisoquinoline

: 147363-24-4
Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / CH₂Cl₂ / 0 °C

2: 68 percent / Na₂CO₃, H₂O / CH₂Cl₂ / 0.08 h

3: 63 percent / CH₂Cl₂

With water; sodium carbonate; In dichloromethane;
DOI:10.1016/S0040-4020(01)80311-2

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 147363-24-4
Paranitrobenzoate de N-methyl-3,4-dihydroisoquinolinium

Guidance literature:: Multi-step reaction with 4 steps

1: 1) aq.KClO 2) benzyltriethylammonium chloride / 1) CH₂Cl₂, 48 deg C, 2) overnight

2: 90 percent / CH₂Cl₂ / 0 °C

3: 68 percent / Na₂CO₃, H₂O / CH₂Cl₂ / 0.08 h

4: 63 percent / CH₂Cl₂

With potassium hypochlorite; N-benzyl-N,N,N-triethylammonium chloride; water; sodium carbonate; In dichloromethane;
DOI:10.1016/S0040-4020(01)80311-2