Technology Process of C30H26O8
There total 10 articles about C30H26O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere
1.2: 25 °C / Inert atmosphere
2.1: copper; copper(II) oxide; dmap / acetonitrile / Inert atmosphere; Reflux
3.1: toluene-4-sulfonic acid / water; isopropyl alcohol / 12 h / Inert atmosphere; Reflux
4.1: toluene-4-sulfonic acid / 1 h / 20 °C / Inert atmosphere; Reflux
5.1: alkaline hydroxide / 12 h / Inert atmosphere; Reflux
5.2: pH 3-4 / Inert atmosphere
With
dmap; copper; toluene-4-sulfonic acid; copper(II) oxide;
In
dichloromethane; water; isopropyl alcohol; acetonitrile;
DOI:10.1002/cjoc.201200977
- Guidance literature:
-
C33H34O9;
for 12h;
Inert atmosphere;
Reflux;
With
hydrogenchloride;
In
water;
pH=3-4;
Inert atmosphere;
DOI:10.1002/cjoc.201200977
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper; copper(II) oxide; dmap / acetonitrile / Inert atmosphere; Reflux
2.1: toluene-4-sulfonic acid / water; isopropyl alcohol / 12 h / Inert atmosphere; Reflux
3.1: toluene-4-sulfonic acid / 1 h / 20 °C / Inert atmosphere; Reflux
4.1: alkaline hydroxide / 12 h / Inert atmosphere; Reflux
4.2: pH 3-4 / Inert atmosphere
With
dmap; copper; toluene-4-sulfonic acid; copper(II) oxide;
In
water; isopropyl alcohol; acetonitrile;
DOI:10.1002/cjoc.201200977