Technology Process of C16H23NO4
There total 5 articles about C16H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / dichloromethane; methanol / 0 °C
2: potassium tert-butylate / isopropyl alcohol / 0 °C
3: dmap / tetrahydrofuran / 20 °C
4: diisobutylaluminium hydride / tetrahydrofuran / -78 - -10 °C
5: pyridinium p-toluenesulfonate
With
dmap; sodium tetrahydroborate; potassium tert-butylate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; isopropyl alcohol;
DOI:10.1016/j.tetasy.2014.02.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / tetrahydrofuran / 20 °C
2: diisobutylaluminium hydride / tetrahydrofuran / -78 - -10 °C
3: pyridinium p-toluenesulfonate
With
dmap; pyridinium p-toluenesulfonate; diisobutylaluminium hydride;
In
tetrahydrofuran;
DOI:10.1016/j.tetasy.2014.02.014
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / dichloromethane; water / 0 °C
2: sodium tetrahydroborate / dichloromethane; methanol / 0 °C
3: potassium tert-butylate / isopropyl alcohol / 0 °C
4: dmap / tetrahydrofuran / 20 °C
5: diisobutylaluminium hydride / tetrahydrofuran / -78 - -10 °C
6: pyridinium p-toluenesulfonate
With
dmap; sodium tetrahydroborate; potassium tert-butylate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.tetasy.2014.02.014
