Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

Base Information

Chemical Name:Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn
CAS No.:1352134-30-5
Molecular Formula:C₄₆H₆₆F₁₂N₆O₉
Molecular Weight:1075.05
Hs Code.:

Synonyms:

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Chemical Property of Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

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Technology Process of Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

There total 13 articles about Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1352134-27-0
C₂₂H₃₅F₆N₃O₆

: 1352134-29-2
C₂HF₃O₂*C₂₄H₃₃F₆N₃O₄

: 1352134-30-5
Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

Guidance literature:: With 4-methyl-morpholine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h;
DOI:10.1002/hlca.201100340

Reference yield:

: 1352134-26-9
Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

: 1352134-30-5
Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 1.5 h / 0 °C

2: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

With 4-methyl-morpholine; HATU; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100340

Reference yield:

: 1352133-79-9
C₂HF₃O₂*C₁₄H₁₉F₂NO₂

: 1352134-30-5
Boc-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-(3S)-β(2,2,3)-hVal(α,α-F2)-(3S)-β(2,2,3)-hAla(α,α-F2)-(3S)-β(2,2,3)-hLeu(α,α-F2)-OBn

Guidance literature:: Multi-step reaction with 5 steps

1: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: dichloromethane / 1.5 h / 0 °C

3: 4-methyl-morpholine; HATU / dichloromethane; N,N-dimethyl-formamide / 12 h / 0 - 20 °C

4: dichloromethane / 1.5 h / 0 °C

5: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

With 4-methyl-morpholine; HATU; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100340