Technology Process of 2-(4-acetamidophenyl)-1,3,2-dithiarsinane
There total 4 articles about 2-(4-acetamidophenyl)-1,3,2-dithiarsinane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
acetic acid;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 0.333333h;
2-(4-aminophenyl)-1,3,2-dithiarsinane;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm500221p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium hydroxide / 0.25 h / 20 °C
2: ethanol / 0.17 h / Reflux
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h
With
ammonium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm500221p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; potassium iodide; sulfur dioxide / methanol; water / 0.5 h / 20 °C
2: ammonium hydroxide / 0.25 h / 20 °C
3: ethanol / 0.17 h / Reflux
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h
With
hydrogenchloride; ammonium hydroxide; sulfur dioxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium iodide;
In
methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm500221p
