trans 2-acetamido-1-phenylselenocyclopentane

Base Information

• Chemical Name: trans 2-acetamido-1-phenylselenocyclopentane
• CAS No.: 77037-13-9
• Molecular Formula: C₁₃H₁₇NOSe
• Molecular Weight: 282.244

Synonyms:

Chemical Property of trans 2-acetamido-1-phenylselenocyclopentane

Chemical Property:

Purity/Quality:

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Technology Process of trans 2-acetamido-1-phenylselenocyclopentane

There total 2 articles about trans 2-acetamido-1-phenylselenocyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

Phenylselenyl chloride (5707-04-0) + cyclopentene (142-29-0) + acetonitrile (75-05-8,26809-02-9) → trans 2-acetamido-1-phenylselenocyclopentane (77037-13-9)

Guidance literature:

With trifluorormethanesulfonic acid; water; for 1h; Heating;

DOI:10.1021/jo00336a021

Reference yield: 66.0%

diphenyl diselenide (1666-13-3) + cyclopentene (142-29-0) + acetonitrile (75-05-8,26809-02-9) → trans 2-acetamido-1-phenylselenocyclopentane (77037-13-9)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; electrolytic process;

DOI:10.1016/0040-4039(80)80190-0

Reference yield:

trans 2-acetamido-1-phenylselenocyclopentane (77037-13-9) → N-cyclopentylacetamide (25291-41-2)

Guidance literature:

With triphenylstannane; In toluene; for 4h; Heating;

DOI:10.1021/jo00336a021

upstream raw materials:

Phenylselenyl chloride

cyclopentene

acetonitrile

diphenyl diselenide

Downstream raw materials:

N-cyclopentylacetamide

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