Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

Base Information

Chemical Name:Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester
CAS No.:142409-36-7
Molecular Formula:C₃₂H₃₈N₄O₁₂P₂
Molecular Weight:732.621
Hs Code.:

Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

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Chemical Property of Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

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Technology Process of Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

There total 7 articles about Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142387-39-1
Phosphoric acid (3aS,4S,5R,6R,7R,7aS)-4,7-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-yl ester bis-(2-cyano-ethyl) ester

: 142409-36-7
Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: With hydrogenchloride; In methanol; acetone; at 20 ℃; for 2h;
DOI:10.1016/S0008-6215(00)90549-4

Reference yield:

: 100-39-0
benzyl bromide

: 142409-36-7
Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1: NaH / dimethylformamide / 20 °C

2: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

3: 530 mg / toluene-p-sulphonic acid / dimethylformamide / 3 h / 20 °C

4: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 1 h / 20 °C

5: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 deg C to 20 deg C

6: 1.8 g / 1 M HCl / acetone; methanol / 2 h / 20 °C

With 1H-tetrazole; hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4

Reference yield:

: 136986-12-4
1,3,4,6-tetra-O-allyl-myo-inositol

: 142409-36-7
Phosphoric acid (1R,2S,3R,4R,5R,6R)-2,5-bis-benzyloxy-6-[bis-(2-cyano-ethoxy)-phosphoryloxy]-3,4-dihydroxy-cyclohexyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1: NaH / dimethylformamide / 20 °C

2: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

3: 530 mg / toluene-p-sulphonic acid / dimethylformamide / 3 h / 20 °C

4: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 1 h / 20 °C

5: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 deg C to 20 deg C

6: 1.8 g / 1 M HCl / acetone; methanol / 2 h / 20 °C

With 1H-tetrazole; hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4