Technology Process of C23H28O4
There total 4 articles about C23H28O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aluminum (III) chloride / dichloromethane / 0 °C
2: bromine / diethyl ether / 1 h / 0 °C
3: potassium hexamethylsilazane / tetrahydrofuran / -78 °C
With
aluminum (III) chloride; bromine; potassium hexamethylsilazane;
In
tetrahydrofuran; diethyl ether; dichloromethane;
1: Friedel Crafts acylation;
DOI:10.1002/cmdc.201000537
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 1 h / 0 °C
2: tetrahydrofuran / 3 h / 0 °C
3: potassium hexamethylsilazane / tetrahydrofuran / -78 °C
With
pyridine; potassium hexamethylsilazane;
In
tetrahydrofuran; dichloromethane;
2: Grignard reaction;
DOI:10.1002/cmdc.201000537
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran / 3 h / 0 °C
2: potassium hexamethylsilazane / tetrahydrofuran / -78 °C
With
potassium hexamethylsilazane;
In
tetrahydrofuran;
1: Grignard reaction;
DOI:10.1002/cmdc.201000537