2--2-(trimethylsilyloxy)cyclobutanon

Base Information

Chemical Name:2--2-(trimethylsilyloxy)cyclobutanon
CAS No.:84629-36-7
Molecular Formula:C₁₇H₂₆O₃Si
Molecular Weight:306.477
Hs Code.:

2-<Hydroxy(2,4,6-trimethylphenyl)methyl>-2-(trimethylsilyloxy)cyclobutanon

Synonyms:

Suppliers and Price of 2--2-(trimethylsilyloxy)cyclobutanon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--2-(trimethylsilyloxy)cyclobutanon

Chemical Property:

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Technology Process of 2--2-(trimethylsilyloxy)cyclobutanon

There total 3 articles about 2--2-(trimethylsilyloxy)cyclobutanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 487-68-3
mesytaldehyde

: 17082-61-0
1,2-bis(trimethylsiloxy)cyclobutene

: 84629-36-7
2--2-(trimethylsilyloxy)cyclobutanon

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 ℃; for 2h; Yield given;

Reference yield:

: 4761-00-6
2,4,6-trimethylbenzylbromide

: 84629-36-7
2--2-(trimethylsilyloxy)cyclobutanon

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / aq. KOH, 2-nitropropane / propan-2-ol / 0.33 h / 40 - 45 °C

2: titanium tetrachloride / CH₂Cl₂ / 2 h / -78 °C

With potassium hydroxide; 2-nitropropane; titanium tetrachloride; In dichloromethane; isopropyl alcohol;

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 84629-36-7
2--2-(trimethylsilyloxy)cyclobutanon

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / NaBr, conc. H₂SO₄ / acetic acid / 8 h / 80 °C

2: 75 percent / aq. KOH, 2-nitropropane / propan-2-ol / 0.33 h / 40 - 45 °C

3: titanium tetrachloride / CH₂Cl₂ / 2 h / -78 °C

With potassium hydroxide; 2-nitropropane; sulfuric acid; titanium tetrachloride; sodium bromide; In dichloromethane; acetic acid; isopropyl alcohol;