2-Fluoro-1-naphthalenecarboxaldehyde

Base Information

• Chemical Name: 2-Fluoro-1-naphthalenecarboxaldehyde
• CAS No.: 82128-49-2
• Molecular Formula: C₁₁H₇FO
• Molecular Weight: 174.174
• Mol file: 82128-49-2.mol

Synonyms:

Chemical Property of 2-Fluoro-1-naphthalenecarboxaldehyde

Chemical Property:

• Melting Point: 64-66°C
• Storage Temp.: -20°C Freezer
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

99%+ ^*data from raw suppliers

2-Fluoro-1-naphthalenecarboxaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Fluoro-1-naphthalenecarboxaldehyde is used in the synthesis of BIPI ligands for asymmetric hydrogenation.

Technology Process of 2-Fluoro-1-naphthalenecarboxaldehyde

There total 1 articles about 2-Fluoro-1-naphthalenecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoronaphthalene (323-09-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2-fluoro-1-naphthaldehyde (82128-49-2) + 2-fluoro-3-naphthaldehyde (21597-61-5)

Guidance literature:

2-fluoronaphthalene; With sec.-butyllithium; at -78 ℃;

N,N-dimethyl-formamide;

DOI:10.1002/mrc.2523

Reference yield: 25.0%

2-fluoro-1-naphthaldehyde (82128-49-2) + salicylaldehyde (90-02-8) → 2-(2-formylphenoxy)-1-naphthaldehyde

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide; for 4h; Reflux;

DOI:10.1039/d0ob02606a

Reference yield:

2-fluoro-1-naphthaldehyde (82128-49-2) → 2-fluoronaphthalen-1-ylmethanol (10336-30-8)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 1h;

upstream raw materials:

2-fluoronaphthalene

N,N-dimethyl-formamide

Downstream raw materials:

2-fluoronaphthalen-1-ylmethanol

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