[((mesityl)N=CPhCMe₂PPh₂)PdMeCl]

Base Information

Chemical Name:[((mesityl)N=CPhCMe₂PPh₂)PdMeCl]
CAS No.:487061-33-6
Molecular Formula:C₃₂H₃₅ClNPPd
Molecular Weight:606.483
Hs Code.:

[((mesityl)N=CPhCMe<sub>2</sub>PPh<sub>2</sub>)PdMeCl]

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Chemical Property of [((mesityl)N=CPhCMe₂PPh₂)PdMeCl]

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Technology Process of [((mesityl)N=CPhCMe₂PPh₂)PdMeCl]

There total 1 articles about [((mesityl)N=CPhCMe₂PPh₂)PdMeCl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.9%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: (mesityl)N=CPhCMe₂PPh₂

: 487061-33-6
[((mesityl)N=CPhCMe₂PPh₂)PdMeCl]

Guidance literature:: In dichloromethane; (Ar); standard Schlenk technique; Pd complex and CH2Cl2 were added to iminephosphine ligand; mixt. was stirred at room temp. for 30 min; evapd.; extd. (hexane); dried; elem. anal.;
DOI:10.1021/om0206305

Reference yield: 94.1%

: 487061-33-6
[((mesityl)N=CPhCMe₂PPh₂)PdMeCl]

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 75-05-8,26809-02-9
acetonitrile

: 487061-37-0
[((mesityl)N=CPhCMe₂PPh₂)Pd(NCMe)Me]B(3,5-C₆H₃(CF₃)2)4

Guidance literature:: In dichloromethane; acetonitrile; byproducts: NaCl; (Ar); standard Schlenk technique; CH3CN and CH2Cl2 were added to mixt. of Pd complex and B compd.; mixt. was stirred at room temp. for 12 h; filtered; evapd.; coevapd. with hexane; elem. anal.;
DOI:10.1021/om0206305

Reference yield:

: 74-85-1
ethene

: 487061-33-6
[((mesityl)N=CPhCMe₂PPh₂)PdMeCl]

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 487061-40-5
[((mesityl)N=CPhCMe₂PPh₂)Pd(ethylene)Me]B(3,5-C₆H₃(CF₃)2)4

Guidance literature:: In dichloromethane-d2; (Ar); standard Schlenk technique; solid Pd complex was mixed with B compd. in NMR tube; cooled to -78°C; ethylene added; CD2Cl2 added; ethylene added; NMR tube was shaken few times and kept at 30°C for 48 h; warmed to room temp.; not isolated; NMR monitoring; Kinetics;
DOI:10.1021/om0206305