Bu₃SNCH(OH)Ph

Base Information Edit

Chemical Name:Bu₃SNCH(OH)Ph
CAS No.:155910-42-2
Molecular Formula:C₁₉H₃₄OSn
Molecular Weight:397.188
Hs Code.:
Mol file:155910-42-2.mol

Synonyms:

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Chemical Property of Bu₃SNCH(OH)Ph Edit

Chemical Property:

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Technology Process of Bu₃SNCH(OH)Ph

There total 2 articles about Bu₃SNCH(OH)Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 10442-39-4
tetra-n-butylammonium cyanide

: 17955-46-3
trimethylsilyltributyltin

: 100-52-7
benzaldehyde

: 155910-42-2,144314-49-8
Bu₃SNCH(OH)Ph

Guidance literature:: In benzene; (Ar); 10°C, 0.6 h, quenching (NH4Cl); extn. (Et2O), washing (HCl), vac. concn.;

Reference yield:

: 688-73-3
tri-n-butyl-tin hydride

: 100-52-7
benzaldehyde

: 155910-42-2,144314-49-8
Bu₃SNCH(OH)Ph

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; under Ar; the Li-amide in THF was added to a soln. of the Sn-hydride in THF at 0°C, stirred for 15 min, cooled to -78°C, addn. of a THF soln. of the aldehyde; quenched after 30 min with NH4Cl soln., extd. with ether, washed with water, dried, concd. in vac.;

Reference yield: 73.0%

: 155910-42-2,144314-49-8
Bu₃SNCH(OH)Ph

: 108-24-7
acetic anhydride

: 1071508-40-1,157339-06-5
(α-(acetyloxy)benzyl)tributylstannane

Guidance literature:: With dmap; triethylamine; In dichloromethane; under Ar; react. in CH2Cl2 for 4-6 h; partitioned between H2O and CH2Cl2, aq. layer was extd. with CH2Cl2, combined organic ext.were washed with brine, dried, volatiles were removed in vac., chromy. on silica gel;