Chol-5-en-24-al-3(beta)-ol

Base Information Edit

Chemical Name:Chol-5-en-24-al-3(beta)-ol
CAS No.:27460-33-9
Molecular Formula:C₂₄H₃₈O₂
Molecular Weight:358.565
Hs Code.:
DSSTox Substance ID:DTXSID601306986
Wikidata:Q105010276
Mol file:27460-33-9.mol

Synonyms:27460-33-9;Chol-5-en-24-al-3(beta)-ol;Vitamin D3 derivative;Chol-5-en-24-al-3beta-ol;Chol-5-en-24-al-3|A-ol;3beta-hydroxychol-5-en-24-al;(4R)-4-[(3S,8S,9S,10R,13R,14S,17R)-3-hydroxy-10,13-dimethyl-2,3,4,7,8,9,11,12,14,15,16,17-dodecahydro-1H-cyclopenta[a]phenanthren-17-yl]pentanal;Chol-5-en-24-al-3b-ol;Chol-5-en-24-al-3??-ol;SCHEMBL10594618;GKTDPIQLKVFPBU-OLSVQSNTSA-N;DTXSID601306986;HY-U00424;(3beta)-3-Hydroxychol-5-en-24-al;AKOS040740746;CS-0035128

Suppliers and Price of Chol-5-en-24-al-3(beta)-ol

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Chol-5-en-24-al-3(beta)-ol Edit

Chemical Property:

XLogP3:5.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:358.287180451
Heavy Atom Count:26
Complexity:581

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CCC=O)C1CCC2C1(CCC3C2CC=C4C3(CCC(C4)O)C)C
Isomeric SMILES:C[C@H](CCC=O)[C@H]1CC[C@@H]2[C@@]1(CC[C@H]3[C@H]2CC=C4[C@@]3(CC[C@@H](C4)O)C)C

Technology Process of Chol-5-en-24-al-3(beta)-ol

There total 6 articles about Chol-5-en-24-al-3(beta)-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 219903-24-9
5-cholenic acid-3β-ol N-methoxy-N-methylamide

: 27460-33-9
3β-hydroxychol-5-en-24-al

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 0.5h;
DOI:10.1021/jo981753v

Reference yield:

: 117886-42-7
3β-hydroxy-cholene-(5)-thioic acid-(24)-S-ethyl ester

: 27460-33-9
3β-hydroxychol-5-en-24-al

Guidance literature:: With nickel; acetone;
DOI:10.1021/ja01189a036

Reference yield:

: 5255-17-4
3β-hydroxy-5-cholenoic acid

: 27460-33-9
3β-hydroxychol-5-en-24-al

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent

2: 94 percent / (CH₃)2AlCl / CH₂Cl₂; hexane / 4 h / Ambient temperature

3: 89 percent / DIBAH / CH₂Cl₂; toluene / 0.5 h / -78 °C

With dimethylaluminum chloride; diisobutylaluminium hydride; In hexane; dichloromethane; toluene;
DOI:10.1021/jo981753v