hexakis-(pentafluoro phenyl) disilane

Base Information

• Chemical Name: hexakis-(pentafluoro phenyl) disilane
• CAS No.: 21094-89-3
• Molecular Formula: C₃₆F₃₀Si₂
• Molecular Weight: 1058.52
• Mol file: 21094-89-3.mol

Synonyms:

Chemical Property of hexakis-(pentafluoro phenyl) disilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hexakis-(pentafluoro phenyl) disilane

There total 9 articles about hexakis-(pentafluoro phenyl) disilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

tris-(pentafluoro phenyl) chloro silane (20160-39-8) + lithium (7439-93-2) → hexakis-(pentafluoro phenyl) disilane (21094-89-3)

Guidance literature:

In diethylene glycol; reaction at 20°C, 24 hours (5 fold excess of Li);;

DOI:10.1007/BF00904310

Reference yield:

tris(pentafluorophenyl)silane (20160-40-1) → hexakis-(pentafluoro phenyl) disilane (21094-89-3)

Guidance literature:

Multi-step reaction with 3 steps

2: tetrahydrofuran

3: diethylene glycol dimethyl ether

In tetrahydrofuran; diethylene glycol dimethyl ether;

Reference yield:

bis-{tris-(pentafluoro phenyl) silyl} mercury (30431-03-9) → hexakis-(pentafluoro phenyl) disilane (21094-89-3)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: diethylene glycol dimethyl ether

In tetrahydrofuran; diethylene glycol dimethyl ether;

upstream raw materials:

tris-(pentafluoro phenyl) chloro silane

lithium

pentafluorophenylmagnesium chloride

tri-(pentafluoro phenyl) dimethylamino silane