O²,O⁴-methanediyl-O¹,O³,O⁵-tris-(toluene-4-sulfonyl)-ribitol

Base Information

• Chemical Name: O²,O⁴-methanediyl-O¹,O³,O⁵-tris-(toluene-4-sulfonyl)-ribitol
• CAS No.: 31320-27-1
• Molecular Formula: C₂₇H₃₀O₁₁S₃
• Molecular Weight: 626.727
• Mol file: 31320-27-1.mol

Synonyms:

Chemical Property of O²,O⁴-methanediyl-O¹,O³,O⁵-tris-(toluene-4-sulfonyl)-ribitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O²,O⁴-methanediyl-O¹,O³,O⁵-tris-(toluene-4-sulfonyl)-ribitol

There total 12 articles about O²,O⁴-methanediyl-O¹,O³,O⁵-tris-(toluene-4-sulfonyl)-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Adonitol (488-81-3) → O2,O4-methanediyl-O1,O3,O5-tris-(toluene-4-sulfonyl)-ribitol (31320-27-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous formaldehyde-solution; aqueous hydrochloric acid

2: pyridine

With pyridine; hydrogenchloride; formaldehyd;

DOI:10.1021/ja01239a033

Reference yield:

D-Arabitol (488-82-4) → O2,O4-methanediyl-O1,O3,O5-tris-(toluene-4-sulfonyl)-D-arabitol (31320-27-1)

Guidance literature:

Multi-step reaction with 4 steps

1: aqueous formaldehyde-solution; aqueous hydrochloric acid

2: pyridine

3: acetic acid anhydride; acetic acid; sulfuric acid / Behandeln des Reaktionsprodukts in Aceton mit wss. Natronlauge

4: pyridine

With pyridine; hydrogenchloride; formaldehyd; sulfuric acid; acetic anhydride; acetic acid;

DOI:10.1021/ja01650a074

Reference yield:

XYLITOL (87-99-0) → O2,O4-methanediyl-O1,O3,O5-tris-(toluene-4-sulfonyl)-xylitol (31320-27-1)

Guidance literature:

Multi-step reaction with 4 steps

1: aqueous hydrochloric acid

2: acetic acid; concentrated sulfuric acid

3: chloroform; sodium methylate; methanol

4: pyridine

With pyridine; hydrogenchloride; methanol; chloroform; sulfuric acid; sodium methylate; acetic acid;

DOI:10.1021/ja01233a002

upstream raw materials:

p-toluenesulfonyl chloride

O²,O⁴-methanediyl-O⁵-(toluene-4-sulfonyl)-D-arabitol

D-Arabitol

O¹,O³;O²,O⁴-dimethanediyl-D-arabitol