methyl N-[[2-methoxy-2-(4-methylphenyl)acetyl]amino]carbamate

Base Information

Chemical Name:methyl N-[[2-methoxy-2-(4-methylphenyl)acetyl]amino]carbamate
CAS No.:119138-37-3
Molecular Formula:C₁₂H₁₆N₂O₄
Molecular Weight:252.27
Hs Code.:
DSSTox Substance ID:DTXSID801144637

Synonyms:119138-37-3;DTXSID801144637;Hydrazinecarboxylic acid, 2-[methoxy(4-methylphenyl)acetyl]-, methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-[[2-methoxy-2-(4-methylphenyl)acetyl]amino]carbamate

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:252.11100700
Heavy Atom Count:18
Complexity:288

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(C(=O)NNC(=O)OC)OC

Technology Process of methyl N-[[2-methoxy-2-(4-methylphenyl)acetyl]amino]carbamate

There total 3 articles about methyl N-[[2-methoxy-2-(4-methylphenyl)acetyl]amino]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 67-56-1
methanol

: 119138-37-3
N'-methoxycarbonyl-2-methoxy-2-p-tolylacetohydrazide

Guidance literature:: With triethylamine; for 1h; Heating;
DOI:10.1016/S0040-4020(01)86184-6

Reference yield: 60.0%

: 127349-86-4
N-<α-(methoxycarbonylhydrazinocarbonyl)-p-methylbenzyl>pyridinium bromide

: 119138-37-3
N'-methoxycarbonyl-2-methoxy-2-p-tolylacetohydrazide

Guidance literature:: With triethylamine; In methanol; for 1h; Heating;

Reference yield:

: 110520-32-6
N'-(2-Bromo-2-p-tolyl-acetyl)-hydrazinecarboxylic acid methyl ester

: 119138-37-3
N'-methoxycarbonyl-2-methoxy-2-p-tolylacetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / acetonitrile / 4 h / Heating

2: 60 percent / NEt₃ / methanol / 1 h / Heating

With triethylamine; In methanol; acetonitrile;