Technology Process of Cyclohexanol, 3-[(phenylmethoxy)methyl]-, cis-
There total 12 articles about Cyclohexanol, 3-[(phenylmethoxy)methyl]-, cis- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: NaH / tetrahydrofuran
2: 1) tert-butyl hydroperoxide, TiCl4, 2) pyridine / 1) CH2Cl2, toluene, -78 deg C, 45 min, 2) room temperature, 12 h
3: 0.70 g / 10percent aq. HCl / aq. ethanol / 0.5 h
4: 0.80 g / t-BuOK / benzene
5: 10 percent Chromat. / LiAlH4 / pentane / 3 h / Ambient temperature
With
pyridine; hydrogenchloride; tert.-butylhydroperoxide; lithium aluminium tetrahydride; potassium tert-butylate; titanium tetrachloride; sodium hydride;
In
tetrahydrofuran; ethanol; pentane; benzene;
DOI:10.1021/jo00031a018
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) tert-butyl hydroperoxide, TiCl4, 2) pyridine / 1) CH2Cl2, toluene, -78 deg C, 45 min, 2) room temperature, 12 h
2: 0.70 g / 10percent aq. HCl / aq. ethanol / 0.5 h
3: 0.80 g / t-BuOK / benzene
4: 10 percent Chromat. / LiAlH4 / pentane / 3 h / Ambient temperature
With
pyridine; hydrogenchloride; tert.-butylhydroperoxide; lithium aluminium tetrahydride; potassium tert-butylate; titanium tetrachloride;
In
ethanol; pentane; benzene;
DOI:10.1021/jo00031a018
- Guidance literature:
-
With
lithium aluminium tetrahydride; (1,4,7,10-tetraoxacyclododecane);
In
pentane;
for 3h;
Title compound not separated from byproducts;
Ambient temperature;
DOI:10.1021/jo00031a018
