L-Valine, N-(N-benzoyl-D-valyl)-, methyl ester

Base Information

Chemical Name:L-Valine, N-(N-benzoyl-D-valyl)-, methyl ester
CAS No.:13795-36-3
Molecular Formula:C₁₈H₂₆N₂O₄
Molecular Weight:334.415
Hs Code.:
Mol file:13795-36-3.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Valine, N-(N-benzoyl-D-valyl)-, methyl ester

Chemical Property:

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Technology Process of L-Valine, N-(N-benzoyl-D-valyl)-, methyl ester

There total 16 articles about L-Valine, N-(N-benzoyl-D-valyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 98-88-4
benzoyl chloride

: 78867-87-5
D-valyl-L-valine methyl ester hydrobromide

: 13795-36-3
N-(N-benzoyl-D-valyl)-L-valine methyl ester

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1039/P19810001639

Reference yield:

: 106561-19-7
Z-D-valyl-D-valine methyl ester

: 13795-36-3,13795-37-4
N-(N-benzoyl-D-valyl)-D-valine methyl ester

Guidance literature:: With palladium; acetic acid; Hydrogenation_.anschliessend Behandeln mit Benzoylchlorid in wss. Na₂CO₃;
DOI:10.1021/ja01160a053

Reference yield:

: 1149-26-4,1685-33-2,92077-76-4,3588-63-4
N-benzyloxycarbonylvaline

: 13795-36-3,13795-37-4
N-(N-benzoyl-D-valyl)-D-valine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅; diethyl ether / Behandeln der Reaktionsloesung mit D-Valin-methylester in Aether und KHCO₃ in H₂O

2: palladium; methanol. acetic acid / Hydrogenation_.anschliessend Behandeln mit Benzoylchlorid in wss. Na₂CO₃

With diethyl ether; phosphorus pentachloride; palladium; acetic acid;
DOI:10.1021/ja01160a053