3-methoxy-4-phenoxylmethylbenzoic acid

Base Information

Chemical Name:3-methoxy-4-phenoxylmethylbenzoic acid
CAS No.:1312583-75-7
Molecular Formula:C₁₅H₁₄O₄
Molecular Weight:258.274
Hs Code.:

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Suppliers and Price of 3-methoxy-4-phenoxylmethylbenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methoxy-4-phenoxylmethylbenzoic acid

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Technology Process of 3-methoxy-4-phenoxylmethylbenzoic acid

There total 2 articles about 3-methoxy-4-phenoxylmethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1373511-82-0
3-methoxy-4-phenoxymethylbromobenzene

: 1312583-75-7
3-methoxy-4-phenoxylmethylbenzoic acid

Guidance literature:: 3-methoxy-4-phenoxymethylbromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/jo300400q

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1312583-75-7
3-methoxy-4-phenoxylmethylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / benzene / 0.17 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 23 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

2.2: 0.25 h / -78 °C / Inert atmosphere

With n-butyllithium; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/jo300400q