5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol

Base Information

Chemical Name:5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol
CAS No.:124211-41-2
Molecular Formula:C₁₅H₂₀O
Molecular Weight:216.323
Hs Code.:

Synonyms:

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Chemical Property of 5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol

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Technology Process of 5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol

There total 8 articles about 5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 57461-21-9,81018-77-1
(3E)-4-(2,3,6-trimethylphenyl)but-3-en-2-one

: 1826-67-1
vinyl magnesium bromide

: 124211-41-2
5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol

Guidance literature:: In tetrahydrofuran;

Reference yield:

: 30316-18-8
1,2-dihydro-3,5,8-trimethyl-naphthalene

: 124211-41-2
5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 1) ozone, 2) water / ethanol, 1) - 80 deg C, 4 h, 2a) 1h, RT, 2b) 30 min, reflux

2: 92 percent / NaBH₄ / methanol / 10 h

3: 95 percent / lithium, liquid ammonia / diethyl ether / 1 h

4: Jones'reagent / acetone / 6 h

5: 92 percent / pyridinium bromide perbromide / tetrahydrofuran / 0.5 h

6: 90 percent / LiBr, Li₂CO₃ / dimethylformamide / 0.75 h / Heating

7: 95 percent / tetrahydrofuran

With sodium tetrahydroborate; Jones'reagent; ammonia; water; pyridinium hydrobromide perbromide; lithium; lithium carbonate; ozone; lithium bromide; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide; acetone;

Reference yield:

: 58720-40-4
4-(2,3,6-trimethyl-phenyl)-butan-2-one

: 124211-41-2
5-(2,3,6-trimethylphenyl)-3-methylpenta-1,4-dien-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / pyridinium bromide perbromide / tetrahydrofuran / 0.5 h

2: 90 percent / LiBr, Li₂CO₃ / dimethylformamide / 0.75 h / Heating

3: 95 percent / tetrahydrofuran

With pyridinium hydrobromide perbromide; lithium carbonate; lithium bromide; In tetrahydrofuran; N,N-dimethyl-formamide;