2,2-Dibenzylcyclopentyl xanthate

Base Information

• Chemical Name: 2,2-Dibenzylcyclopentyl xanthate
• CAS No.: 147779-81-5
• Molecular Formula: C₂₁H₂₄OS₂
• Molecular Weight: 356.553
• Mol file: 147779-81-5.mol

Synonyms:

Chemical Property of 2,2-Dibenzylcyclopentyl xanthate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2-Dibenzylcyclopentyl xanthate

There total 2 articles about 2,2-Dibenzylcyclopentyl xanthate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dibenzylcyclopentanone (57772-75-5) → 2,2-Dibenzylcyclopentyl xanthate (147779-81-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.70 g / LiAlH₄ / diethyl ether / 1 h / Heating

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/jo00062a043

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 2,2-dibenzylcyclopentanol (147779-80-4) + methyl iodide (74-88-4) → 2,2-Dibenzylcyclopentyl xanthate (147779-81-5)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jo00062a043

Reference yield:

2,2-Dibenzylcyclopentyl xanthate (147779-81-5) → 8-Benzyl-10-bromo-6,7,8,9-tetrahydro-5H-5,8-methano-benzocycloheptene

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / 1 h / 1) 145-165 deg C, 1 h, 2) 160-170 deg C, 0.5 h

2: 79 percent / Br₂ / CCl₄ / 0.08 h / 0 °C

With bromine; In tetrachloromethane;

DOI:10.1021/jo00062a043

upstream raw materials:

carbon disulfide

2,2-dibenzylcyclopentanol

methyl iodide

2,2-dibenzylcyclopentanone

Refernces