3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide

Base Information

Chemical Name:3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide
CAS No.:120657-78-5
Molecular Formula:C₁₂H₁₇N
Molecular Weight:175.274
Hs Code.:

Synonyms:

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Chemical Property of 3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide

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Technology Process of 3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide

There total 1 articles about 3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 73494-01-6
3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl bromide

: 544-92-3
copper(I) cyanide

: 120657-78-5
3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide

Guidance literature:: In dimethyl sulfoxide; 40 deg C, 1 h; 85 deg C 2 h;

Reference yield:

: 120657-78-5
3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide

: 120657-81-0
4-(4'-methylcyclohex-3'-en-1-yl)pent-3-en-1-al

Guidance literature:: Multi-step reaction with 3 steps

1: 1) HCl gas, 2, H₂O / 1) H₂O, reflux, 2) H₂O, 100 deg C, 20 min

2: 70 percent / LiAlH₄ / diethyl ether / 3 h / Heating

3: 68 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

With pyridine; chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; water; In diethyl ether; dichloromethane;

Reference yield:

: 120657-78-5
3-(4'-methylcyclohex-3'-en-1-yl)but-2-enyl cyanide

: 29837-07-8
(Z)-α-bisabolene

Guidance literature:: Multi-step reaction with 4 steps

1: 1) HCl gas, 2, H₂O / 1) H₂O, reflux, 2) H₂O, 100 deg C, 20 min

2: 70 percent / LiAlH₄ / diethyl ether / 3 h / Heating

3: 68 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

4: 1) NaH / 1) DMSO, 2) DMSO, THF, 2 h, RT then 50 deg C, 30 min and overnight, RT

With pyridine; chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; water; sodium hydride; In diethyl ether; dichloromethane;