Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)

Base Information

Chemical Name:Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)
CAS No.:358970-99-7
Molecular Formula:C₃₇H₄₀NO₅P₃Ru₂
Molecular Weight:873.79
Hs Code.:

Ru<sub>2</sub>(CO)4(NO)(P(C(CH<sub>3</sub>)3)2)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)

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Technology Process of Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)

There total 1 articles about Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: tetrafluoroboric acid

: 225092-99-9
[Ru2(CO)4(μ-H)(μ-P(t)Bu2)(μ-dppm)]

: 80-11-5
N-methyl-N-nitrosotoluene-p-sulfonamide

: 358970-99-7
Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)

: 358971-05-8
Ru₂(CO)4(H)2(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Ru₂(CO)4(H)2(P(C₄H₉)2)((C₆H₅)2PCH₂P(C₆H₅)2)]BF₄

Guidance literature:: In 1,4-dioxane; under Ar; Schlenk technique; Ru complex dissolved in dioxane, soln. treated with nitrosyl compd.; stirred at reflux for 2 h; cooled to room temp.; solvent removed in vac.; residue dissolved in Et2O; filtered through Al2O3; eluate treated with hexane; elem. anal.;
DOI:10.1002/zaac.201100226

Reference yield: 80.0%

: tetrafluoroboric acid

: 358970-99-7
Ru₂(CO)4(NO)(P(C(CH₃)3)2)((C₆H₅)2PCH₂P(C₆H₅)2)

: 262280-70-6
Ru2(CO)4(μ-H)(μ-NO)(.mum-P(t-Bu)2)(μ-dppm)

Guidance literature:: In diethyl ether; Schlenk technique; under Ar; to Et2O soln. of Ru complex, added Et2O soln. of HBF4 with stirring; stirred for 30 min; ppt. filtered off, washed with Et2O several times; recrystd. from CH2Cl2/Et2O; elem. anal.;
DOI:10.1002/zaac.201100226