<6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt

Base Information

Chemical Name:<6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt
CAS No.:139263-66-4
Molecular Formula:C₁₂H₂₇N*C₃₃H₂₉N₅O₆S₂
Molecular Weight:841.108
Hs Code.:

<6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt

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Technology Process of <6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt

There total 1 articles about <6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-82-9
tributyl-amine

: 139263-65-3
<6R<6α,7β(Z)>>-3-(acetoxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) triethylamine salt

: 139263-66-4
<6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt

Guidance literature:: With sodium hydroxide; In methanol; at -25 - -20 ℃; for 1h; Yield given;
DOI:10.1055/s-1992-26326

Reference yield:

: 79660-72-3
fleroxacin

: 139263-66-4
<6R<6α,7β(Z)>>-3-(hydroxymethyl)-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid (1:1) tributylamine salt

: N-((2R,2aR)-1,7-Dioxo-2,2a,5,7-tetrahydro-1H,4H-6-oxa-3-thia-7b-aza-cyclobuta[e]inden-2-yl)-2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetamide

: 139263-67-5
<6R<6α,7β(Z)>>-3-<<6,8-difluoro-1-(2-fluoroethyl)-1,4-dihydro-7-(4-methyl-1-piperazinyl)-4-oxo-3-quinolinyl>carbonyloxymethyl>-7-<(methoxyimino)<2-(triphenylmethyl)amino-4-thiazolyl>acetylamino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxyli...

Guidance literature:: With tributyl-amine; cyclohexyl chloroformate; dmap; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH2Cl2, -25 deg C, 2.) CH2Cl2, a) -25 deg C, 2 h, b) -25 -> 0 deg C, 1.5 h;
DOI:10.1055/s-1992-26326