Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

Base Information

Chemical Name:Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate
CAS No.:53807-44-6
Molecular Formula:C₃₀H₃₂CrO₄*F₆P
Molecular Weight:653.542
Hs Code.:

Synonyms:

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Chemical Property of Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

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Technology Process of Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

There total 1 articles about Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: ferrocenium hexafluorophosphate

: 53807-42-4
Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6)

: 53807-44-6
Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

Guidance literature:: In dichloromethane; N2; addn. of iron complex salt to dichloromethane soln. of Cr complex, stirring for 10 min; pptn. by addn. of hexane and reduction of vol. in vac., washing the solid with n-hexane;

Reference yield: 57.0%

: 53807-44-6
Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

: 824-11-3
ethriol phosphite

: 507491-25-0
Cr(CO)(P(OCH2)3CC2H5)(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

Guidance literature:: In dichloromethane; N2; addn. of ligand to a stirred dichloromethane soln. of Cr complex, stirring for 2 h; addn. of n-hexane, reducing the solvent in vac., washing with n-hexane, dissolving in CH2Cl2, filtering through Celite, addn. of hexane, pptn. by reduction of solvent in vac.; elem. anal.;

Reference yield: 39.0%

: 53807-44-6
Cr(CO)2(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

: 121-45-9
phosphorous acid trimethyl ester

: 507491-27-2
Cr(CO)(trimethoxyphosphine)(η-(H3COC6H4)CC(C6H4OCH3))(η-C6(methyl)6) hexafluorophosphate

Guidance literature:: In dichloromethane; N2; addn. of ligand to a stirred dichloromethane soln. of Cr complex, stirring for 2 h; addn. of n-hexane, reducing the solvent in vac., washing with n-hexane, dissolving in CH2Cl2, filtering through Celite, addn. of hexane, pptn. by reduction of solvent in vac.; elem. anal.;