PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

Base Information

Chemical Name:PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂
CAS No.:932015-65-1
Molecular Formula:C₁₉H₂₃ClNO₂PPd
Molecular Weight:470.244
Hs Code.:

PdClCH<sub>3</sub>(CH<sub>3</sub>)2C<sub>3</sub>H<sub>2</sub>NOCOP(C<sub>6</sub>H<sub>5</sub>)2H<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

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Technology Process of PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

There total 1 articles about PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 932015-63-9
1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 932015-65-1
PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

Guidance literature:: In dichloromethane; (under N2, Schlenk); Pd-complex added to CH2Cl2 soln. of ligand at room temp., stirred overnight; solvent evapd. under reduced pressure, ppt. washed with Et2O, pentane, dried under vac.; elem. anal.;
DOI:10.1039/b616962g

Reference yield: 82.0%

: 932015-65-1
PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

: 2923-28-6
silver trifluoromethanesulfonate

: 932015-67-3
PdCF₃SO₃CH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

Guidance literature:: In dichloromethane; byproducts: AgCl; (under N2, Schlenk); AgCF3SO3 added to CH2Cl2 soln. of Pd-complex, stirred at room for 2 h protected from light; filtered, solvent evapd. under reduced pressure, residue washed with Et2O, pentane, dried under vac.; elem. anal.;
DOI:10.1039/b616962g