α-Cyano-β-aminocrotonamide

Base Information

Chemical Name:α-Cyano-β-aminocrotonamide
CAS No.:103607-64-3
Molecular Formula:C₁₂H₁₃N₃O₂
Molecular Weight:231.254
Hs Code.:

α-Cyano-β-<N-(p-methoxyphenyl)>aminocrotonamide

Synonyms:

Suppliers and Price of α-Cyano-β-aminocrotonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-Cyano-β-aminocrotonamide

Chemical Property:

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Technology Process of α-Cyano-β-aminocrotonamide

There total 1 articles about α-Cyano-β-aminocrotonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 62321-92-0
α-cyano-β-dimethylaminocrotonamide

: 104-94-9
4-methoxy-aniline

: 103607-64-3,120651-01-6
α-Cyano-β-aminocrotonamide

Guidance literature:: In acetic acid; Heating;
DOI:10.1007/BF00767827

Reference yield:

: 103607-64-3,120651-01-6
α-Cyano-β-aminocrotonamide

: 103589-62-4
2-(3-Isopropyl-2-phenyl-oxazolidin-5-ylmethoxy)-4-(4-methoxy-phenylamino)-nicotinonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 3 h / Heating

2: 1 N NaOH / 1 h / Heating

3: 68 percent / POCl₃, dimethylaniline / 2 h / Heating

4: 18-crown-6, KOH / toluene / 6 h / Heating

With potassium hydroxide; sodium hydroxide; 18-crown-6 ether; 2,3-Dimethylaniline; trichlorophosphate; In ethanol; toluene;
DOI:10.1007/BF00767827

Reference yield:

: 103607-64-3,120651-01-6
α-Cyano-β-aminocrotonamide

: 2-(2-Hydroxy-3-isopropylamino-propoxy)-4-(4-methoxy-phenylamino)-nicotinonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol / 3 h / Heating

2: 1 N NaOH / 1 h / Heating

3: 68 percent / POCl₃, dimethylaniline / 2 h / Heating

4: 18-crown-6, KOH / toluene / 6 h / Heating

5: aq. HCl / 2 h / 50 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; 18-crown-6 ether; 2,3-Dimethylaniline; trichlorophosphate; In ethanol; toluene;
DOI:10.1007/BF00767827